HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 68140643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 21503457 | HCID 21503457 | — |
| Reactant | HCID 54416263 | HCID 54416263 | — |
| Product | HCID 68140643 | HCID 68140643 | 16% |
Reaction Steps
9-Hydroxy-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester hydrochloride was prepared from 9-hydroxy-1,2,4,5-tetrahydro-11-methyl-3H-azepino[4,5-b]quinoline and ethyl chloroformate analogous to Example 63, followed by hydrolysis of the intermediate 9-(ethoxy-carbonyloxy)-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester with dilute potassium hydroxide at 30° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-23f52f61032f4b6e85e38083c6c5643f |
| Source note | uspto-grants-1976_10 |