Ethyl chloroformate → HCID 68139021, compound

HRID 1288135Notes

Reaction equation

HRID 1288135 reaction equation
[CH3:1][C:2]1[C:11]2[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=2[N:5]=[C:4]2[CH2:12][CH2:13][CH2:14][NH:15][CH2:16][C:3]=12.[Cl:17][C:18]([O:20][CH2:21][CH3:22])=[O:19]>>[ClH:17].[CH2:21]([O:20][C:18]([N:15]1[CH2:14][CH2:13][CH2:12][C:4]2=[N:5][C:6]3[CH:7]=[CH:8][CH:9]=[CH:10][C:11]=3[C:2]([CH3:1])=[C:3]2[CH2:16]1)=[O:19])[CH3:22]

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 3044001HCID 3044001, compound

Product 1

HCID 68139021HCID 68139021, compoundYield 58%

Procedure

2,3,4,5-Tetrahydro-11-methyl-1H-2-azepino[4,3-b]quinoline-carboxylic acid ethyl ester hydrochloride was prepared from 2,3,4,5-tetrahydro-11-methyl-1H-azepino[4,3-b]quinoline and ethyl chloroformate analogous to Example 63.

Sources & evidence

ORD record
ord-3232a7443e5e4869912cb26c90b68d74
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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