Ethyl chloroformate → HCID 68140112, compound

HRID 1288136Notes

Reaction equation

HRID 1288136 reaction equation
[CH2:1]1[C:15]2[C:6](=[N:7][C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=3[CH:14]=2)[CH2:5][CH2:4][CH2:3][NH:2]1.[Cl:16][C:17]([O:19][CH2:20][CH3:21])=[O:18]>>[ClH:16].[CH2:20]([O:19][C:17]([N:2]1[CH2:3][CH2:4][CH2:5][C:6]2=[N:7][C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=3[CH:14]=[C:15]2[CH2:1]1)=[O:18])[CH3:21]

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 215034522,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline

Product 1

HCID 68140112HCID 68140112, compoundYield 81%

Procedure

2,3,4,5-Tetrahydro-1H-2-azepino[4,3-b]quinoline-carboxylic acid ethyl ester hydrochloride was prepared from 2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline and ethyl chloroformate analogous to Example 63.

Sources & evidence

ORD record
ord-87b0592692fa417999bc58f3ddb107df
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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