Phenyl chloroformate → HCID 54533678, compound

HRID 1288141Notes

Reaction equation

C([N:3]1[CH2:18][CH2:17][CH2:16][C:6]2=[N:7][C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=3[C:14]([Cl:15])=[C:5]2[CH2:4]1)C.Cl[C:20]([O:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1)=[O:21]>>[C:23]1([O:22][C:20]([N:3]2[CH2:18][CH2:17][CH2:16][C:6]3=[N:7][C:8]4[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=4[C:14]([Cl:15])=[C:5]3[CH2:4]2)=[O:21])[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

Reactant 2

HCID 15891Phenyl chloroformate

HCID 21503410HCID 21503410, compound

Product 1

HCID 54533678HCID 54533678, compoundYield 18.5%

Procedure

11-Chloro-2,3,4,5-tetrahydro-1H-2-azepino[4,3-b]quinoline-carboxylic acid phenyl ester was prepared analogous to Example 98 from 2-ethyl-11-chloro-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline and phenyl chloroformate.

Sources & evidence

ORD record: ord-4ae9166ff1ce4f07a087414c06ae2053
Source dataset: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03987047

Reaction notes

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