Acetyl chloride → HCID 21503385, compound

HRID 1288147Notes

Reaction equation

HRID 1288147 reaction equation
[CH3:1][C:2]1[C:11]2[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=2[N:5]=[C:4]2[CH2:12][CH2:13][CH2:14][NH:15][CH2:16][C:3]=12.[C:17]([Cl:20])(=[O:19])[CH3:18]>>[ClH:20].[C:17]([N:15]1[CH2:14][CH2:13][CH2:12][C:4]2=[N:5][C:6]3[CH:7]=[CH:8][CH:9]=[CH:10][C:11]=3[C:2]([CH3:1])=[C:3]2[CH2:16]1)(=[O:19])[CH3:18]

Participants

3

Reactant 2

HCID 6367Acetyl chlorideHCID 3044001HCID 3044001, compound

Product 1

HCID 21503385HCID 21503385, compoundYield 75%

Procedure

2-Acetyl-2,3,4,5-tetrahydro-11-methyl-1H-azepino[4,3-b]quinoline hydrochloride was prepared from 2,3,4,5-tetrahydro-11-methyl-1H-azepino[4,3-b]quinoline and acetyl chloride analogous to Example 63.

Sources & evidence

ORD record
ord-198b98dac859492fbe8fad3dcabd1b63
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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