HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 21503593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 3044012 | HCID 3044012 | — |
| Reactant | HCID 21503466 | HCID 21503466 | — |
| Product | HCID 21503593 | HCID 21503593 | 79% |
Reaction Steps
2-Acetyl-5-hydroxy-11-methyl-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline hydrochloride was prepared from 5-hydroxy-11-methyl-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline and acetyl chloride analogous to Example 63, followed by hydrolysis of the intermediate 2-acetyl-5-acetoxy-2,3,4,5-tetrahydro-11-methyl-1H -azepino[4,3-b]quinoline with dilute sodium hydroxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-e4892135f4ac49d785a3dc41989ccfec |
| Source note | uspto-grants-1976_10 |