HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 21503466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 21503643 | HCID 21503643 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21503466 | HCID 21503466 | — |
Reaction Steps
A mixture of 3 gm (11 millimols) of 2-acetyl-2,3,4,5-tetrahydro-11-methyl-1H-azepino[4,3-b]quinoline 6-oxide, 80 ml of benzene and 23 ml of acetic acid anhydride was heated at its boiling point for 3 hours. Thereafter, the benzene was distilled off and the residue ws recrystallized from ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-30f2baf61684461688e0223c02aacad2 |
| Source note | uspto-grants-1976_10 |