Ethyl chloroformate → HCID 54491737, compound

HRID 1288164Notes

Reaction equation

HRID 1288164 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][C:5]2[C:6]([CH3:17])=[C:7]3[CH2:16][NH:15][CH2:14][CH2:13][CH2:12][C:8]3=[N:9][C:10]=2[CH:11]=1.Cl[C:19]([O:21][CH2:22][CH3:23])=[O:20]>>[CH2:22]([O:21][C:19]([N:15]1[CH2:14][CH2:13][CH2:12][C:8]2=[N:9][C:10]3[CH:11]=[C:2]([CH3:1])[CH:3]=[CH:4][C:5]=3[C:6]([CH3:17])=[C:7]2[CH2:16]1)=[O:20])[CH3:23]

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 21503456HCID 21503456, compound

Product 1

HCID 54491737HCID 54491737, compoundYield 42%

Procedure

8,11-Dimethyl-2,3,4,5-tetrahydro-1H-2-azepino[4,3-b]quinoline-carboxylic acid ethyl ester was prepared from 8,11-dimethyl-2,3,4,5-tetrahydro-1H-azepino[4,3-b]quinoline and ethyl chloroformate analogous to Example 155.

Sources & evidence

ORD record
ord-0b57a5653dc247beb6063b2d35e6fbff
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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