Ethyl chloroformate → HCID 68139184, compound

HRID 1288168Notes

Reaction equation

HRID 1288168 reaction equation
[CH3:1][C:2]1[C:11]2[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=2[N:5]=[C:4]2[CH:12]=[CH:13][NH:14][CH2:15][CH2:16][C:3]=12.[Cl:17][C:18]([O:20][CH2:21][CH3:22])=[O:19]>>[ClH:17].[CH2:21]([O:20][C:18]([N:14]1[CH2:15][CH2:16][C:3]2[C:4](=[N:5][C:6]3[CH:7]=[CH:8][CH:9]=[CH:10][C:11]=3[C:2]=2[CH3:1])[CH:12]=[CH:13]1)=[O:19])[CH3:22]

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 21503525HCID 21503525, compound

Product 1

HCID 68139184HCID 68139184, compoundYield 42%

Procedure

1,2-Dihydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester hydrochloride was prepared from 1,2-dihydro-11-methyl-3H-azepino[4,5-b]quinoline and ethyl chloroformate analogous to Example 155.

Sources & evidence

ORD record
ord-caf68294340e4b96aa702550fca0e642
Source dataset
uspto-grants-1976_10
Patent number
US03987047

Reaction notes

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