HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 54204945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 21503606 | HCID 21503606 | — |
| Product | HCID 54204945 | HCID 54204945 | 92% |
Reaction Steps
1,2,4,5-Tetrahydro-11-methyl-7-trifluoromethyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester was prepared from 1,2,4,5-tetrahydro-11-methyl-7-trifluoromethyl-3H-azepino[4,5-b]quinoline and ethyl chloroformate analogous to Example 155. Yield: 92% of theory; m.p. 136° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03987047 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-1e43af1f4fdb4a739b2132c37f339389 |
| Source note | uspto-grants-1976_10 |