HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 317170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1H-Indole-3-carboxylic acid, 2-chloro-1-methyl- | HCID 99522 | — |
| Product | HCID 317170 | HCID 317170 | 67% |
Reaction Steps
Similar reaction of 2-chloro-1-methylindole-3-carboxylic acid [XXI] with SOCl2 and N-methylaniline gave N-methyl-N-phenyl 2-chloro-1-methylindole-3-carboxamide [XXII: R6 =Me; R7 =Ph] (67% yield); mp (Me2CO/water) 163° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464861 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-d9c115f2a7c24c609e764cc843cbe50f |
| Source note | uspto-grants-1995_11 |