HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 14943551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 1-(Benzenesulfonyl)-1H-indole-3-carbonyl chloride | HCID 2776211 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14943551 | HCID 14943551 | — |
Reaction Steps
Reaction of 3-chlorocarbonyl-1-(phenylsulfonyl)-indole [XXIII] (Ketcha D. M., Gribble G. W., J. Org. Chem. 1985;50:5451-5457) with an excess of benzylamine in CH2Cl2) (method of Ketcha and Gribble) gave N-benzyl-1-(phenylsulfonyl) indole-3-carboxamide [XXIV: R8 =CH2Ph]; mp (MeOH) 188°-189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05464861 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-872931821d894614af45e6097663593a |
| Source note | uspto-grants-1995_11 |