Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Thiophosphoryl chloride | HCID 19883 | — |
| Product | Phenylthionophosphonic dichloride | HCID 19016 | — |
Reaction Steps
In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03988368 |
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| Source dataset | uspto-grants-1976_10 |
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| ORD ID | ord-3415756249a948d698066d8c2ad191f4 |
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| Source note | uspto-grants-1976_10 |
|---|
