Methyl iodide → HCID 54096469, compound

Participants

Reaction Steps

The same procedure as in Example A-1 was repeated except that 2,34 g of diethyl 2-heptenephosphonate and 1.42 g of methyl iodide were used instead of 1.92 g of the diethyl 2-butenephosphonate and 1.7 g of the benzyl bromide respectively. Vacuum distillation of the reaction mixture afforded 2.23 g of diethyl 1-methyl-2-heptene-phosphonate having a boiling point of 128° C. (3 mmHg) in a yield of 90%.

Provenance & Evidence