Methyl iodide → HCID 21502530, compound

Participants

Reaction Steps

To a solution of [1-methyl-3-(2,6,6-trimethyl-1-cyclohexenyl)propyl]dimethylamine (2.0 g) in dry ether (20 cc) was added methyliodide (2.0 g), and the mixture was allowed to stand overnight. Precipitated crystals were gathered by filtration and recrystallized from a mixed solvent of ethanol, benzene and ether to give colorless crystals (3.0 g) of [1-methyl-3-(2,6,6-trimethyl-1-cyclohexenyl)propyl]trimethylammonium iodide, m.p. 220°-222° C.

Provenance & Evidence