Methyl iodide → HCID 21502479, compound

Participants

Reaction Steps

A solution of [3-(2,6,6-trimethyl-1-cyclohexenyl)-2(trans)-propenyl]dimethylamine (2.0 g) in dry ether (20 cc) was added to methyliodide (2.0 g), and the reaction mixture was allowed to stand over night. Precipitated crystals were gathered by filtration, and recrystallized from a mixed solvent of ethanol, benzene and ether to give colorless crystals (2.3 g) of [3-(2,6,6-trimethyl-1-cyclohexenyl)-2(trans)-propenyl]trimethylammonium iodide, m.p. 180° C.

Provenance & Evidence