Methanol → HCID 21502543, compound

Participants

Reaction Steps

A solution of [3-(2,6,6-trimethyl-1-cyclohexenyl)-2(trans)-propenyl]dimethylamine (2.0 g) and propargylbromide (2.0 g) in methanol (20 cc) was refluxed for 1 hour, and concentrated. To the residue was added water, and the aqueous solution was washed with ether and extracted with chloroform. The chloroform layer was dried and concentrated to dryness to give an oil (2.9 g) of [3-(2,6,6-trimethyl-1-cyclohexenyl)-2(trans)-propenyl]dimethylpropargylammonium bromide.

Provenance & Evidence