HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2-(Chloromethyl)-6-methylnaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Naphthalenemethanol, 6-methyl- | HCID 3015042 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-(Chloromethyl)-6-methylnaphthalene | HCID 13301557 | — |
Reaction Steps
20.3 g. of 6-methyl-2-naphthalenemethanol is dissolved in 100 ml. of dry benzene and to this solution is added 30 ml. of thionyl chloride. The solution is stirred for about one hour and concentrated to yield 2-chloromethyl 6-methylnaphthalene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03988457 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-be97f8851ab442e2a31052c5e03f4ac4 |
| Source note | uspto-grants-1976_10 |