HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Vinylpyridine → HCID 135840377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Vinylpyridine | HCID 7502 | — |
| Reactant | 52119-95-6 | HCID 3711484 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 135840377 | HCID 135840377 | — |
Reaction Steps
A solution of 6.6 g (0.062 mol) 4-vinylpyridine and 14.1 g (0.05 mol) 3,5-di-t-butyl-4-hydroxydithiobenzoic acid in 50 ml toluene was refluxed for 6 hours. On cooling, the product (via anti-Markovnikov addition) crystallized from the reaction mixture. After recrystallization from chloroform, the product melted at 191°-193° C. Elemental analysis of the product is tabulated in Table I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03988471 |
| Source dataset | uspto-grants-1976_10 |
| ORD ID | ord-b4f4784f4d6142c99786a9b3ebd11c78 |
| Source note | uspto-grants-1976_10 |