化工社化工社 化学情報印刷レポート · 研究参考用
Nitric Acid → 2-Nitro-5-phenyl indane-1,3-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Nitric Acid | HCID 944 | — |
| 反応物 | 5-Phenyl indane-1,3-dione | HCID 22345836 | — |
| 生成物 | 2-Nitro-5-phenyl indane-1,3-dione | HCID 21503064 | — |
反応手順
Nitration of 5-phenyl indane-1,3-dione with fuming nitric acid as described in Example 16 (c) gave 2-nitro-5-phenyl indane-1, 3-dione, m.p. (water, hydrochloric acid) 119° C. (Found: C, 65.54; H, 3.39; N, 4.93; C15H9NO4. 1/2 H2O requires: C, 65.21; H, 3.65; N, 5.07%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03988476 |
| 出典データセット | uspto-grants-1976_10 |
| ORD ID | ord-ee77cc7bd0b64510831b47ca317bdae4 |
| 出典メモ | uspto-grants-1976_10 |