Sodium Iodide → HCID 14662926, compound

Participants

Reaction Steps

The crude product produced in Example V is dissolved in 6 ml of acetic acid with 0.1 g of sodium iodide. By GLC on Carbowax(polyethylene glycol), it is clear that the 1,1-dimethoxy-cis-3-hexene-2-one is converted to a new material of later retention time. After 1/2 hour less than 5 percent of "cis" material remains.

Provenance & Evidence