HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54536067, compound → HCID 15410466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54536067 | HCID 54536067 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 15410466 | HCID 15410466 | 87% |
Reaction Steps
A solution of 2.15 g of 5,6-dihydro-5-(4-nitrobenzoyl)phenanthridine in 50 ml of ethyl acetate and 0.5 g of 10% palladium-on-carbon is hydrogenated in a Parr apparatus under an atmosphere of hydrogen for three hours. The mixture is filtered through diatomaceous earth and the solvent removed to give 1.7 g of the product as a yellow foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05747487 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-389c96b047fa40acb0300d2cb1987b6e |
| Source note | uspto-grants-1998_05 |