4-Bromoanisole → HCID 54068620, compound

HRID 1289055Notes

Reaction equation

HRID 1289055 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([O:8][CH3:9])=[CH:4][CH:3]=1.[C:10]([C:13]1[S:17][C:16]([CH3:18])=[N:15][C:14]=1[CH3:19])(=[O:12])[CH3:11]>>[CH3:9][O:8][C:5]1[CH:6]=[CH:7][C:2]([C:10]([C:13]2[S:17][C:16]([CH3:18])=[N:15][C:14]=2[CH3:19])([OH:12])[CH3:11])=[CH:3][CH:4]=1

Participants

3

Reactant 2

HCID 77304-BromoanisoleHCID 5208882,4-Dimethyl-5-acetylthiazole

Product 1

HCID 54068620HCID 54068620, compound

Procedure

Following the general method of Example 3 but starting with 4-bromoanisole and 5-acetyl-2,4-dimethylthiazole, the title compound was prepared. M.p. 114-115.5° C.

Sources & evidence

ORD record
ord-896533d0d0424f17846e6a98841546ce
Source dataset
uspto-grants-1998_05
Patent number
US05747515

Reaction notes

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