HRID1289073

反应详情

EQUATION

反应方程式

HRID 1289073 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

After dissolving 0.5 g of 2-nitro-3-(4-tolyl)thiophene in 20 ml of dioxane, 0.25 g of 5% pd/C was added and catalytic reduction was carried out at room temperature for 5 hours. The solution obtained was filtered to recover the catalyst and the filtrate was used as intact for the next reaction.

WORKUP

后处理

  1. additionpd/C was added
  2. customThe solution obtained
  3. filtrationwas filtered
  4. customto recover the catalyst
  5. customintact for the next reaction