HCID 18925390, compound → 3-(4-Chlorophenyl)-2-thiophenamine
Reaction equation
[N+](C1SC=CC=1C1C=CC(C)=CC=1)([O-])=O.[N+:16]([C:19]1[S:20][CH:21]=[CH:22][C:23]=1[C:24]1[CH:29]=[CH:28][C:27]([Cl:30])=[CH:26][CH:25]=1)([O-])=O>>[NH2:16][C:19]1[S:20][CH:21]=[CH:22][C:23]=1[C:24]1[CH:25]=[CH:26][C:27]([Cl:30])=[CH:28][CH:29]=1Participants
3
Procedure
The same procedures as described in Example 1 were carried out except that 2-nitro-3-(4-tolyl)thiophene was replaced by 2-nitro-3-(4-chlorophenyl)thiophene, and the filtrate thus obtained was used as intact for the next reaction.
Workup
- customthe filtrate thus obtained
- customintact for the next reaction
Sources & evidence
- ORD record
- ord-8460b675529f4d2c9189cec6f7972b24
- Source dataset
- uspto-grants-1998_05
- Patent number
- US05747518
Reaction notes
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