HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 9837462, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | HCID 18920440 | HCID 18920440 | — |
| Product | HCID 9837462 | HCID 9837462 | — |
Reaction Steps
5,5'-Dihydroxymethyl-2,2'-bithiophene was also obtained by refluxing 2-hydroxy-methyl-5-iodo-thiophene with Cu powder in dimethyl formamide. The Ullmann condensation yielded a very poor amount of 5,5'-dihydroxymethyl-2,2'-bithiophene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05747525 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-d1ab307bd2174ff18ef9295134da764f |
| Source note | uspto-grants-1998_05 |