HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 69956186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 18921781 | HCID 18921781 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69956186 | HCID 69956186 | 57.3% |
Reaction Steps
After N-methylaniline(0.9 ml, 8.4 mmol) was added to a mixture solution of 6-methyl-4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(1.5 g, 5.5 mmol) and dimethylformamide(10 ml), 1.2 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-6546070fa0c649e3b5b6e3caffa31974 |
| Source note | uspto-grants-1998_05 |