HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Toluidine → HCID 18921661, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Toluidine | HCID 7242 | — |
| Reactant | HCID 18921765 | HCID 18921765 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921661 | HCID 18921661 | 62.1% |
Reaction Steps
After 2-methylaniline(0.46 ml, 4.31 mmol) was added to a mixture solution of 6-ethyl-4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(0.61 g, 2.12 mmol) and dimethylformamide(5 ml), 0.52 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-4086e533c5504056b6a2c5e1c9dd1b80 |
| Source note | uspto-grants-1998_05 |