HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 69954405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 54298114 | HCID 54298114 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69954405 | HCID 69954405 | 29% |
Reaction Steps
After N-methylaniline(1.04 ml, 9.6 mmol) was added to a mixture solution of (R)-5,6-dimethyl-4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(1.4 g, 4.8 mmol) and dimethyl formamide(10 ml), 0.55 g of the title compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-9ed4d2b0533c4a2d8d912fe282c74a75 |
| Source note | uspto-grants-1998_05 |