HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 18921713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | HCID 18921662 | HCID 18921662 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921713 | HCID 18921713 | 50.3% |
Reaction Steps
After 4-fluoroaniline(0.50 ml, 5.28 mmol) was added to a mixture solution of 5-methyl-6-ethyl-4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine (0.80 g, 2.65 mmol) and dimethylformamide(5 ml), 0.55 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-44e9b49c8a4b4905850a4dd36de2dea8 |
| Source note | uspto-grants-1998_05 |