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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1289525Generated: October 31, 2026

N-Methylaniline → HCID 69955429, compound

https://huagongshe.com/reaction/1289525

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-MethylanilineHCID 7515—
ReactantHCID 18921662HCID 18921662—
SolventDimethylformamideHCID 6228—
ProductHCID 69955429HCID 6995542955.4%

Reaction Steps

After N-methylaniline(0.44 ml, 4.06 mmol) was added to a mixed solution of 5-methyl-6-ethyl-4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(0.80 g, 2.65 mmol) and dimethylformamide(5 ml), 0.60 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05750531
Source datasetuspto-grants-1998_05
ORD IDord-6ceab82d405e48429e057dcac9e4f188
Source noteuspto-grants-1998_05