HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 69955429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 18921662 | HCID 18921662 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69955429 | HCID 69955429 | 55.4% |
Reaction Steps
After N-methylaniline(0.44 ml, 4.06 mmol) was added to a mixed solution of 5-methyl-6-ethyl-4-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(0.80 g, 2.65 mmol) and dimethylformamide(5 ml), 0.60 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-6ceab82d405e48429e057dcac9e4f188 |
| Source note | uspto-grants-1998_05 |