HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-methylaniline → HCID 18921722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Reactant | HCID 18921782 | HCID 18921782 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921722 | HCID 18921722 | 58.1% |
Reaction Steps
After 2-methyl-4-fluoroaniline(0.8 ml, 7.2 mmol) was added to a mixture solution of 6-methyl-4-(1,2,3,4-tetrahydroisoquinoline-2-yl)-2-chloropyrimidine(1.0 g, 3.8 mmol) and dimethylformamide(10 ml), 0.85 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-cb68403464f04f76ab1b45f6ed72306c |
| Source note | uspto-grants-1998_05 |