HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 69956241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 18921782 | HCID 18921782 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69956241 | HCID 69956241 | 52.3% |
Reaction Steps
After N-methylaniline(0.61 ml, 5.48 mmol) was added to a mixture solution of 6-methyl-4-(1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloropyrimidine(0.95 g, 3.65 mmol) and dimethylformamide(10 ml), 0.7 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-f6a95462a58e49b486dae9ea80d67fc2 |
| Source note | uspto-grants-1998_05 |