HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-methylaniline → HCID 18921717, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Reactant | HCID 18921761 | HCID 18921761 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921717 | HCID 18921717 | 28.2% |
Reaction Steps
After 4-fluoro-2-methylaniline(0.75 ml, 6.6 mmol) was added to a mixture solution of 4-(1,2,3,4-tetrahydroisoquinolin-2-yl)-2-chloro-5,6,7,8-tetrahydroquinazoline(0.90 g, 3.0 mmol) and dimethylformamide(5 ml), 0.36 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-bd9eece3683b44cca28ddbab1de4d413 |
| Source note | uspto-grants-1998_05 |