HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoro-2-methylaniline → HCID 18921723, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoro-2-methylaniline | HCID 67982 | — |
| Reactant | HCID 18921720 | HCID 18921720 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921723 | HCID 18921723 | 14.4% |
Reaction Steps
After 4-fluoro-2-methylaniline(0.51 ml, 4.59 mmol) was added to a mixture solution of 5-methyl-4-(7-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridin-6-yl)-6-ethyl-2-chloropyrimidine(0.74 g, 2.4 mmol) and dimethylformamide(5 ml), 0.15 g of the titled compound was obtained in accordance with the same procedure as in Step 2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-87ee19293fee43ac9e9e47db3117b379 |
| Source note | uspto-grants-1998_05 |