HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 18921745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | HCID 18921675 | HCID 18921675 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18921745 | HCID 18921745 | 52% |
Reaction Steps
After 4-fluoroaniline(0.8 ml, 8.4 mmol) was added to a mixture solution of 6-methyl-2-(1-methyl-1,2,3,4-tetrahydroisoquinolin-2-yl)-4-chloropyrimidine(1.5 g, 5.5 mmol) and dimethylformamide(10 ml), 1.1 g of the titled compound was obtained in accordance with the same procedure as in Step 4 of Example 57.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-0f4c9f4bf874419aa2a9824809e63302 |
| Source note | uspto-grants-1998_05 |