HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → HCID 67627932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | HCID 18921734 | HCID 18921734 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67627932 | HCID 67627932 | 20% |
Reaction Steps
After N-methylaniline(0.5 ml, 4 mmol) was added to a mixture solution of 5,6-dimethyl-2-(7-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridin-6-yl)-4-chloropyrimidine(0.64 g, 2 mmol) and dimethylformamide(10 ml), 0.16 g of the titled compound was obtained in accordance with the same procedure as in Step 4 of Example 57.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750531 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-fc48b075b32948c5b4b107aa9f51be0e |
| Source note | uspto-grants-1998_05 |