Methyl iodide → HCID 19075402, compound
Reaction equation
[CH3:1][I:2].[CH2:3]([S:5][C:6]1[C:10]([C:11]2[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=2)=[N:9][S:8][N:7]=1)[CH3:4]>>[I-:2].[CH2:3]([S:5][C:6]1[C:10]([C:11]2[CH:12]=[N+:13]([CH3:1])[CH:14]=[CH:15][CH:16]=2)=[N:9][S:8][N:7]=1)[CH3:4]Participants
3
Procedure
Methyl iodide (0.5 ml, 7.5 mmol) was added to a solution of 3-(3-ethylthio-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.
Workup
- customevaporated
Sources & evidence
- ORD record
- ord-529c81fa76744505bb4521c02c0646e9
- Source dataset
- uspto-grants-1998_05
- Patent number
- US05750541
Reaction notes
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