HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1289764Generated: November 1, 2026
Methanol → Naphthalenecarboxylic acid, methyl ester
https://huagongshe.com/reaction/1289764
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1-Naphthoic acid | HCID 6847 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | Naphthalenecarboxylic acid, methyl ester | HCID 120056 | 87% |
Reaction Steps
The synthesis method of Example 7-(1) was applied. 1--Naphthoic acid (4.97 g), methanol (10 ml), 1,2-dichloroethane (12 ml) and concentrated sulfuric acid (0.6 ml) were used as reagents and the mixture was stirred at 60° C. for 17 hours. After the reaction, the mixture was extracted with ether to give 4.35 g of a pale-yellow transparent liquid (yield 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05750545 |
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| Source dataset | uspto-grants-1998_05 |
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| ORD ID | ord-d31b0986991a4eab84e50f179c483f9d |
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| Source note | uspto-grants-1998_05 |
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