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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1289764Generated: November 1, 2026

Methanol → Naphthalenecarboxylic acid, methyl ester

https://huagongshe.com/reaction/1289764

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantSulfuric AcidHCID 1118—
Reactant1-Naphthoic acidHCID 6847—
Solvent1,2-DichloroethaneHCID 11—
ProductNaphthalenecarboxylic acid, methyl esterHCID 12005687%

Reaction Conditions

Temperature60 °C

Reaction Steps

The synthesis method of Example 7-(1) was applied. 1--Naphthoic acid (4.97 g), methanol (10 ml), 1,2-dichloroethane (12 ml) and concentrated sulfuric acid (0.6 ml) were used as reagents and the mixture was stirred at 60° C. for 17 hours. After the reaction, the mixture was extracted with ether to give 4.35 g of a pale-yellow transparent liquid (yield 87%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05750545
Source datasetuspto-grants-1998_05
ORD IDord-d31b0986991a4eab84e50f179c483f9d
Source noteuspto-grants-1998_05