HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → Methyl 3-(4-chlorophenyl)-2-propenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 2-Propenoic acid, 3-(4-chlorophenyl)- | HCID 15371 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 3-(4-chlorophenyl)-2-propenoate | HCID 98955 | 95% |
Reaction Steps
The synthesis method of Example 7-(1) was applied. 4-Chlorocinnamic acid (10.0 g), 1,2-dichloroethane (50 methanol (9.0 ml) and concentrated sulfuric acid (0.4 ml) were used as reagents to give 10.2 g of a white solid (yield 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750545 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-0677265866c244d1aee9377bcdf37155 |
| Source note | uspto-grants-1998_05 |