Trimethyl orthobeznoate → HCID 10514375, compound

Participants

Reaction Steps

The synthesis method of Example 96 was applied. The compound (1.50 g) obtained in Example 29 and trimethylorthobenzoate (5.0 ml) were used. The mixture was reacted at 150° C. for 2 hours. The resulting crystals were collected by filtration and purified by a method similar to the method of Example 98, whereby crystals (1.53 mg) were obtained (yield 66%). The crystals were recrystallized from methanol to give colorless transparent plate crystals.

Provenance & Evidence