HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70197051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54060679 | HCID 54060679 | — |
| Reactant | HCID 70193605 | HCID 70193605 | — |
| Reactant | HCID 70195376 | HCID 70195376 | — |
| Product | HCID 70197051 | HCID 70197051 | — |
Reaction Steps
By steps analogous to steps (a) to (c) of Synthetic Example 14, the product from step (a) was converted to (R)-3-(1-methyl -1,2,3,6-tetrahydro-4-pyridyl)-5-(2-oxo-1,3-oxazolidin-4-ylmethyl) -1H-indole hydrate, mp 229°-231° C., [α]D18 +24.9° (c=0.5, IN aqu. HCl). Elemental analysis and 1H NMR were consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05466699 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-722bc40db5d4489182d916a7b7727dd8 |
| Source note | uspto-grants-1995_11 |