Methanol → HCID 67593132, compound

Participants

Reaction Steps

A solution of 275 mg of product from Step C in 5 mL of methanol and 0.5 mL of TTA was stirred with 100 mg of 10% Pd/C under a hydrogen balloon for 60 h. The reaction was filtered and concentrated. The residue was purified by flash chromatography eluting with 5 to 10% methanol in methylene chloride to obtain 220 mg of title compound. T.l.c. (5% methanol in methylene chloride) Rf =0.25. Mass spec (NH3 /CI): 262 (M+1).

Provenance & Evidence