HCID 18922532, compound → HCID 18922462, compound

Participants

Reaction Steps

A solution of 90 mg of the product from Step E in 5 mL of methanol was hydrogenated over 25 mg of 10% Pd/C at 40 psi for 2 h and then filtered and evaporated. The residue was purified by flash chromatography eluting with 1% NH4OH/10% methanol in methylene chloride to obtain 20 mg of title compound. T.l.c. (5% methanol in methylene chloride) Rf =0.1.

Provenance & Evidence