2-Hydroxy-1,2,3-propanetricarboxylic acid hydrate (1:1) → HCID 178485755, compound

Participants

Reaction Steps

The compound (300 mg) obtained in Example 1 was dissolved in ethyl acetate (3 ml) and a solution of citric acid monohydrate (92.7 mg) in ethyl acetate (5 ml) was dropwise added. After stirring at room temperature for 15 minutes, crystals were collected by filtration and dried under reduced pressure to give 257 mg of the title compound as white crystals (see Table 16).

Provenance & Evidence