HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzene, 1-chloro-3-isocyanato- → 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzene, 1-chloro-3-isocyanato- | HCID 17968 | — |
| Edukt | N-nitroimidazolidin-2-imine | HCID 135413413 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine | HCID 136342791 | — |
Reaktionsschritte
A solution of 3.9 g of 2-nitroiminoimidazolidine and 4.6 g of 3-chlorophenylisocyanate in 80 ml of dry acetonitrile was refluxed for 3 hours. After cooling to room temperature, the precipitated crystals were filtered, and washed with ether to give desired 1-(3-chlorophenylcarbamoyl)-2-nitroiminoimidazolidine. The yield was 4.7 g.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05750704 |
| Quelldatensatz | uspto-grants-1998_05 |
| ORD ID | ord-b6a48d70c56741a78504a7c935926eae |
| Quellennotiz | uspto-grants-1998_05 |