HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 18923724, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3,5-Dichloro-N-methylaniline | HCID 12377757 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 18923724 | HCID 18923724 | — |
Reaction Steps
The mixture of 3,5-dichloro-N-methylaniline (345 mg) and excess amount of benzyl bromide and triethylamine in acetonitrile (7 ml) was refluxed for 4 hours. The reaction mixture was separated with ethyl acetate and water, and the organic layer was washed with water, dried and concentrated in vacuo to give N-benzyl-3,5-dichloro-N-methylaniline (532 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750699 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-b35469c020ae486fa123b4406c5b2a24 |
| Source note | uspto-grants-1998_05 |