Dichloromethane → HCID 13679341, compound

HRID 1290247Notes

Reaction equation

HRID 1290247 reaction equation
[C:1]1([CH2:7][CH2:8][C:9](=[O:11])[CH3:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl[CH2:13]Cl>>[O:11]1[C:9]([CH3:13])([CH2:8][CH2:7][C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:10]1

Participants

3

Reactant 2

HCID 6344DichloromethaneHCID 17355Benzyl acetone

Product 1

HCID 13679341HCID 13679341, compoundYield 72%

Procedure

Using the same conditions described in Example 5, but using dichloromethane as the extraction solvent, 4-phenyl-2-butanone (22.2 g, 0.15 mole) yielded an orange oil; 1,2-epoxy-2-methyl-4-phenylbutane (19.8 g, 72% yield of theory).

Workup

  1. customyielded an orange oil

Sources & evidence

ORD record
ord-4272bb3247ed4d5d9069753d7180a156
Source dataset
uspto-grants-1998_05
Patent number
US05750740

Reaction notes

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