HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl nitrate → HCID 10981608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl nitrate | HCID 15575 | — |
| Reactant | HCID 10640035 | HCID 10640035 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10981608 | HCID 10981608 | — |
Reaction Steps
17β-cyclopropyloxy-androst-4-en-3-one (9.70 g, 29.5 5 mM), potassium tert-butoxide (7.0 g, 62.4 mM), and isopropyl nitrate (2.99 ml) are reacted by the method of Example 1 to yield 17β-cyclopropyloxy-4-nitroandrost-4-en-3-one, m.p. 137°-38° C. (methanol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750744 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-f5192f0f302044c6a3579430a2ed098d |
| Source note | uspto-grants-1998_05 |