HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosgene → 4-(Chloromethyl)-2,5-oxazolidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosgene | HCID 6371 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 45086566 | HCID 45086566 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 4-(Chloromethyl)-2,5-oxazolidinedione | HCID 21764295 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 50 using 1.24 g of 2-chloro-L-alanine, 16 ml of 1.93M phosgene in toluene and 55 ml of tetrahydrofuran to give 0.150 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05750735 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-2a679c3e489c4e0793fc0d76a95aa970 |
| Source note | uspto-grants-1998_05 |